Industrial organic chemistry and catalysis practical

Uitgebreide vaknaam	Industrial organic chemistry and catalysis practical
Leerdoelen	At the end of the course, the student is able to: 1. Plan and perform (catalytic) organic chemical transformation based on literature procedures under specified conditions (e.g. anhydrous) 2. Select, plan and carry out work up procedures including separation and purification using different techniques (e.g. column chromatography, distillation, acid-base extraction and crystallization) 3. Select and perform adequate chemical analysis techniques, and interpret the data to identify the outcome of experiments 4. Carry out laboratory procedures in a safe and responsible manner 5. Log and report experimental details and results at the level common in scientific publications and based on appropriate theory on catalytic and organic reaction mechanism that would enable another researcher to reproduce the experiment
Omschrijving	The students will carry out 5-6 synthesis protocol experiments and one multi-day project which involves the (catalytic) synthesis of organic molecules and study of their properties or optimize reaction parameters. Within the project there is room for the development of the student’s own ideas. Experiments and the project need to be prepared in a lab book and discussed with the teaching assistants and the results need to be recorded in the lab book and documented in a report. The students are expected to run multiple experiments in parallel.
Uren per week
Onderwijsvorm	Hoorcollege (LC), Practisch werk (PRC) (Workload: Selfstudy 20 hrs, Lecture 2 hrs, Protocol experiments 62 hrs, Mini research project 56 hrs)
Toetsvorm	Practisch werk (PR), Verslag (R) (Report (50%) Practical (50%). See remarks.)
Vaksoort	bachelor
Coördinator	Prof. Dr. P. Raffa
Docent(en)	T.R. Canrinus, PhD. ,prof. dr. P.J. Deuss , N.N.H.M. Eisink, PhD. ,Prof. Dr. P. Raffa
Verplichte literatuur	Titel Auteur ISBN Prijs Student manual
Entreevoorwaarden	Prerequisite: Practical Synthesis and Analysis 1
Opmerkingen	Pass mark: The average of the marks for each experiment should be over 5.5. Student get quizzed before experiments and are monitored in the laboratory by TA's. They are provide feedback halfway the course on the progress and on their first report(s). The final grade is given based on performance in the second half and their final project report. Attendance is compulsory for all parts of the course The course unit assumes prior knowledge acquired from earlier courses in the curriculum of BSc Chemical Engineering in particular Industrial Organic Chemistry and Catalysis as well as Synthesis 1 and Organic Chemistry 1.
Opgenomen in	Opleiding Jaar Periode Type BSc Chemical Engineering 2 semester I b verplicht Pre-master/Fast-track for MSc Chemistry - CE  (Pre-master Chemical Engineering) - semester I b verplicht Pre-master/Fast-track for MSc Chemistry - CE  (Pre-master Chemical Engineering for IEM students) - semester I b verplicht Pre-master/Fast-track for MSc Chemistry - CE  (Fast-track Chemical Engineering) - semester I b verplicht